Make Essential Oils

Essential oils are highly concentrated oils extracted from aromatic plants like lavender and rosemary. About 700 different kinds of plants contain useful essential oils, and there are several methods employed to extract them — the most common of which is distillation. While essential oils can be very expensive to buy, they are relatively cheap to distill at home.

Steps

Setting Up Your Essential Oil Still

  1. Purchase an essential oil still. Although you’ll likely be hard-pressed to find one in a store (unless you have a specialty store nearby), these stills are easy to buy online. However, beware that they can be expensive — usually around a couple hundred dollars. If you plan on making large quantities of essential oil, a professional still is a good investment.
  2. Build your own still if you don’t want to buy one. If you want to try building a still, you've got plenty of room for creativity - there are thousands of still designs, and even today, many stills are homemade. The key components of a still are:
    • A heat source — usually direct fire
    • A pressure cooker
    • A 10 mm glass pipe
    • A tub of cold water to cool down and condense the steam flowing through the pipe[1]
    • An essencier, which separates out the essential oil from other materials you don’t want in your final product.[2]
  3. Use stainless steel and glass parts, if possible.[3] Do not use plastic tubing in place of a glass pipe, as it can affect the quality of the oil. Some plants react badly with copper, but heavily tinned copper is suitable in all cases. You can also use aluminum materials, but not with wintergreen, cloves, or other plants whose oils have phenols.
  4. Bend the pipe so it can pass through the cooling tub. You’ll bring the plant matter to heat in the pressure cooker, and the resulting steam will pass through the pipe. You have to be able to cool that steam back down to liquid by immersing it in a cold water or ice bath. Depending on what you’re using for your cooling tub, you’ll have to bend the pipe in different shapes. For example, if you’re simply using a basin, you might have to bend it into a coil so that it can lay in the open tub. If you’re using a large bucket of ice, you might be able to bend the pipe to a 90 degree angle so that it can go down through the top of the bucket, then out a hole in the bottom.
  5. Connect the pipe to the pressure cooker valve. Use a small piece of flexible hose that fits snugly over both openings, which should be roughly the same size if you’re using a 10 mm pipe. You can secure the connection using a jubilee clip purchased at a hardware store.
    • Make sure you cut the hose long enough to allow some room to bend. Otherwise, your pipe will stick straight up in the air, and you’ll have to give it a 90 degree bend so it can run toward the cooling tub.
  6. Run the pipe through the cooling tub. If you’re using an open basin, position it so that the coil lies completely inside the tub. It should be completely submerged when the basin is filled with cold water or ice. If you’re using a bucket, drill a small hole in the bottom so the pipe can pass out of the ice bath. Seal the hole using a silicone sealer or epoxy to prevent water from dripping through it and making a mess.
  7. Position the open end of the pipe over the essencier. Once the distillate drips into the essencier, it will do all the rest of the work for you. It will separate the essential oil from the rest of the matter that you don’t want in your final product.
  8. Make sure all your instruments are in stable positions. Depending on the tools you’re using and the shape of your pipe, you may have to work a little bit to find a safe, stable setup for all of your still components. Put the lid on the pressure cooker with the pipe attached to it, run the pipe through your cooling tub, and position the open end of the pipe over your essencier. Make sure the pipe is at a comfortable angle and nothing will get knocked over.

Preparing Your Plant Material

  1. Determine when to harvest your plant material. The amount of oil in a plant depends on where it is in its life cycle, so it’s important to harvest each species of plant at the right time. You need to do some research to figure out when to harvest the plants you want to distill. For example, lavender should be harvested when about half the flowers on the stem have withered.[4] Rosemary, on the other hand, should be harvested when the plants are in full bloom.[5]
  2. Harvest your plants correctly. Just as you need to research when to harvest plants for best essential oil production, you need to research how to harvest them. Careless handling, harvesting the wrong parts, even harvesting at the wrong time of day can reduce the quantity and quality of the essential oils. For example, you only want to use the flowering tops of the rosemary plant when making rosemary essential oil. Discard or use the rest of the plant some other way.
    • Most essential oils are held in the plant's oil glands, veins and hairs, and these are very fragile. If you disturb or break them, you’ll get less oil from your plants. Handle the plants with care, and handle them as little as possible.
  3. Be choosy if purchasing your plants. If you're buying already-harvested plants, you will not have much control over the harvesting process. Look for plants that appear healthy and undamaged, and ask the seller when they were harvested. Generally, plants that are in whole form (not crushed or powdered) are best.
    • While distillation removes many impurities, pesticides and herbicides can contaminate your oil. It’s best to use organically grown plants, whether you purchase them or grow your own.
  4. Dry the plant material. Drying reduces the amount of oil in each plant, but can greatly increase how much essential oil you make per batch. This is because you’ll be able to fit more material into each batch. Drying should be done slowly and away from direct sunlight.[6] Commercially grown plants such as lavender and peppermint may be allowed to dry in the field after cutting for a day or so.
    • The ideal drying method varies from plant to plant, but in general, you shouldn’t overheat the plants. Drying in the shade or even in a dark room minimizes the oil loss.
    • Don’t allow the plants to become wet again before distillation. Distill as soon as possible after drying.
    • You can choose not to dry your plant material if you’d like to skip this step.

Distilling Your Essential Oil

  1. Pour water into the tank of your still. If you made your own still, your tank is the pressure cooker. Use clean water; it should be ideally filtered or distilled and as soft as possible. If you're using a manufactured still, follow the manufacturer's direction. Otherwise, just make sure you have enough water to complete the distillation. Depending on the plant and on the quantity, distillation can take anywhere from a half-hour to six hours or more after the water boils.
  2. Add your plant matter to the water. Fit as much plant matter as the tank can contain. As long as you have enough water to last without boiling off, your plants should be fine even if they’re packed in tight. Just make sure that they don’t block the steam outlet in the lid of the pressure cooker.[7] Give yourself a couple inches of leeway.
    • You don’t need to chop or otherwise prepare the plant in any way — in fact, doing so will cause you to lose some of the oils.
  3. Bring the pressure cooker to a boil. Seal the lid so that the only steam that escapes must travel through the pipe that’s attached to the steam valve. Most plants will release their essential oils at 100 degrees Celsius or 212 degrees Fahrenheit — the normal boiling point of water.[8]
  4. Keep an eye on the still. After a while, the distillate should begin to come through your condenser and into your separator. The process should be fairly hands-off, but you want to make sure you don’t run out of water in your still. Depending on the length of the distillation process, you may also need to change the water in the cold-water tub. If the hot pipe warms the water up, replace it with fresh cold water or ice so that the cooling process continues to work.
  5. Filter the collected oil (optional). Once your distillation is complete, you might choose filter the oil through cheesecloth or similar dry cotton fabric. Make sure that the cloth is dry and clean — detergent residues and dirt can contaminate the oil.
    • Don’t be disappointed that you get a very small amount of essential oil from a large amount of plant matter. Percent yields vary from species to species, but they’re always lower than a beginning distiller might think.[9]
  6. Pour the oil into a container for storage as quickly as possible. Most essential oils can be kept for at least one or two years, but some have very short shelf lives.[10] To maximize the useful life of your oil, keep it in a dark glass bottle or stainless steel container. Use a clean funnel to pour the oil into the container, and make sure the container is clean before pouring the oil into it. Store it in a cool, dark place.[11]
    • Decide what to do with the hydrosol as well. The other material in the essencier is hydrosol — water that’s been distilled and infused with the scent of the plant.
    • Some hydrosols, like rose or lavender water are usable themselves.
    • If you don’t want to save the hydrosol, you can pour it into the still for the next batch if you will be distilling another batch immediately. Otherwise, throw it out.

Tips

  • Essential oils are extremely concentrated, and it is often advisable to dilute them in a carrier oil before applying them to skin. The most popular carrier oils are almond oil and grapeseed oil, but a variety of different oils can be used. They can be added during the bottling process or mixed with the pure oil just prior to use. The latter is often preferable because you may not want diluted oil for some uses, and carrier oils often have a shorter shelf life than essential oils.

Warnings

  • Most essential oils should not be ingested, especially if undiluted, and many should be diluted even when applied topically. Also, some essential oils are toxic. See the external links for more information.
  • For the distillation of most flowers, skip the drying process and distill soon after harvesting.
  • Do not distill a batch for too long (check recommendations for the specific plant), as this will add little additional oil but may possibly contaminate your batch with unwanted chemical compounds.
  • If the plant is organic, that does not mean that pesticides or fertilizers were not applied to it; they are just different from commonly used synthetic pesticides or fertilizers (which some are less toxic than types of organics). Try to find a local grower who can inform you about how the plant was grown.
  • When drying plant material, you should exercise care not to allow the material to become contaminated with dirt, dust or other contaminants. Contamination will reduce the quality of your oil and may make it unusable.

Things You'll Need

  • Distillation equipment, including at least a tank, a condenser, a furnace or other heat source and a separator.
  • Glass tubing to connect distillation components
  • Plant materials from which to extract the oils
  • Containers made of dark glass or stainless steel in which to store the oils

Related Articles

Sources and Citations

  1. ↑ Krell, Erich Handbook of Laboratory Distillation. New York: Elsevier Science Ltd., 1981.
  2. ↑ http://www.essentialoil.com/products/glass-essencier-essential-oil-separator
  3. ↑ Krell, Erich. Handbook of Laboratory Distillation. New York: Elsevier Science Ltd., 1981.
  4. ↑ http://www.millbrooklavenderfarm.com/lavender/harvesting-lavender
  5. ↑ http://www.nda.agric.za/docs/Brochures/ProGuiRosemary.pdf
  6. ↑ http://www.researchgate.net/publication/233842808_Drying_Method_Affects_Essential_Oil_Content_and_Composition_of_Basil_(Ocimum_basilicum_L.)
  7. ↑ http://www.b-ecochic.com/how-to-make-essential-oils.html
  8. ↑ https://www.naha.org/explore-aromatherapy/about-aromatherapy/how-are-essential-oils-extracted/
  9. ↑ http://www.essentialoil.com/pages/percentage-yield
  10. ↑ http://www.aromaweb.com/articles/essentialoilshelflife.asp
  11. ↑ http://www.quinessence.com/shelf_life.htm
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